Thermofisher Quanta 3D

Q3D Manual

Electron optics

 

  • High resolution Schottky field emission
  • SEM column optimized for high brightness/high current
  • 60° objective lens geometry with through- the-lens differential pumping and heated objective apertures
  • Maximum horizontal field width: 5 mm at analytical working distance (10 mm); 18.8mm at 65 mm WD;
  • Accelerating voltage: 200 V to 30 kV
  • Landing voltage range: Standard: 200 V to 30 kV, Beam Deceleration: 20 V to 30 kV
  • Probe current: ≤ 200 nA, continuously adjustable
  • Magnification: 30 to 1 450 kx

 

Electron Beam resolution

 

  • High vacuum

0.8 nm at 30 kV (STEM)

1..2 nm* at 30 kV (SE)

2.5 nm at 30 kV (BSE)

2.9 nm at 1 kV (SE)

  • High vacuum with beam deceleration option

3.0 nm at 1 kV (BD mode + BSED)

2.3 nm at 1 kV (BD mode + ICD)

3.1 nm at 200 V (BD mode + ICD)

  • Low vacuum

1.5 nm at 30 kV (SE)

2.5 nm at 30 kV (BSE)*

2.9 nm at 3 kV (SE)

  • Extended vacuum mode (ESEM)

1.5 nm at 30 kV (SE)

 

Detectors

 

  • Everhardt Thornley SED (secondary electron detector)
  • Low vacuum SED
  • Gaseous SED (GSED) (used in ESEM mode)
  • Gaseous analytical BSED (GAD)
  • Gaseous BSED
  • Solid State backscatter detector BSED
  • 14 segment STEM detector
  • In-column detector (ICD) for BD mode
  • EDS
  • EBSD

 

Vacuum system

 

  • Patented through-the-lens differential pumping
  • Beam gas path length: 10 mm or 2 mm
  • 2 x IGP
  • Chamber vacuum (high) < 6e-4 Pa
  • Chamber vacuum (low) < 10 to 130 Pa
  • ESEM vacuum < 10 to 4000 Pa
  • Evacuation time: 150 seconds to high vacuum and  270 seconds to ESEM
  • CryoCleaner cold trap

 

Accessories

 

  • SW controlled Peltier cooled specimen stage
  • SW controlled 1000°C heating stage
  • SW controlled 1400°C heating stage
  • FEI Gas Injection System: Platinum
  • Prototyping: Integrated 16-bit patterning engine
  • Integrated Plasma Cleaner

 

Chamber

  • 379 mm size left to right
  • 10 mm analytical WD E and I beam coincidence point
  • 21 ports
  • EDS take-off angle: 35°
  • Angle between electron and ion columns 52

 

Stage

 

  • X, Y = 50 mm
  • Z = 25 mm
  • Z clearance = 50 mm
  • T = - 15° to + 75°
  • R = 360° continuous

 

Ion Optics

 

  • High-current ion column with Ga liquid-metal ion source
  • Acceleration voltage: 2-30kV
  • Probe current 1pA-65 nA in 15 steps
  • Beam blanker
  • 15 position aperture strip
  • Magnification: 30 to 1 450 kx
  • Charge neutralization mode for milling of non-conductive samples

 

Ion  Beam resolution

 

-   7 nm at 30 kV at beam coincident point